Departmental Bulletin Paper マイクロ波を用いたN-メチル-N-フェニルカルバモイルクロリドの合成と反応
Synthesis and reaction of N-methyl-N-phenylcarbamoyl chloride using microwaves

鈴木, 常夫  ,  種村, 潔

Description
N-methy-N-phenylcarbamoyl chloride was synthsized by the reaction of N-methylformanilide and thionyl chloride under microwave irradiation. By the treatment of N-methyl-N-phenylcarbamoyl chloride with sodium ethoxide and N-methylaniline ethyl N-methyl-N-phenylcarbamate and N,N'-dimethyl N,N'-diphenylurea was obtained, respectively.
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